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Synopsis Efficient use of analytical instruments requires an understanding of the fundamental principles and techniques upon which modern measuring devices are based. Only then one can make intelligent choice among the many possible ways of solving an analytical problem; and appreciate the pitfalls that accompany an physical measurements. The present publication allows the reader to find information about the analytical instrumental techniques that are commonly used to provide information on chemical composition and structure. This publication is divided into four sections i.e., Introduction, Spectroscopy, Chromatography and Miscellaneous Methods. The publication has been written keeping in view the latest syllabi of several Indian universities. The subject matter, both as regards the arrangement of chapters as well as the contents of each chapter has been so graded, proceeding from simple to more difficult topics, that a student may follow the course with great ease and interest. The method of presentation is very clear and lucid. It is our earnest hope that this edition will be of great value to all our students.